| THE STRUCTURE OF TETRABUTYLAMMONIUM BIS(1,3-DITHIO-2-THION-CYCLOPENTENE-4, 5-DITHIOLATE)PALLADIUM(Ⅱ) |
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| 摘 要： | <正> Mr=984.05 monoclinic P21/c a=8.474(1),b=14.768(3), c=19.494(3) A,6=96.42(1)0, V=2424.5(7)A3, Z=2, (Mokα)=8.Hem-1, F(000)=1039.91, room temperature. The final R=0.0357 for 2696 independant reflections. The Pd(C3S5)22-ion is nearly planar and the Palladium(Ⅱ)-sulfur coordination polyhedron is square planar with Pd-S distances of 2.315A and 2.311A.
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THE STRUCTURE OF TETRABUTYLAMMONIUM BIS(1,3-DITHIO-2-THION-CYCLOPENTENE-4, 5-DITHIOLATE)PALLADIUM(Ⅱ) |
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| Abstract: | Mr=984.05 monoclinic P21/c a=8.474(1),b=14.768(3), c=19.494(3) A,6=96.42(1)0, V=2424.5(7)A3, Z=2, (Mokα)=8.Hem-1, F(000)=1039.91, room temperature. The final R=0.0357 for 2696 independant reflections. The Pd(C3S5)22-ion is nearly planar and the Palladium(Ⅱ)-sulfur coordination polyhedron is square planar with Pd-S distances of 2.315A and 2.311A. |
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