| 共沉淀法制备YAG粉体影响因素研究 |
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| 引用本文： | 罗军明,邓莉萍. 共沉淀法制备YAG粉体影响因素研究[J]. 无机化学学报, 2010, 26(2): 240-244 |
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| 作者姓名： | 罗军明 邓莉萍 |
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| 作者单位： | 南昌航空大学材料科学与工程学院,南昌,330063 |
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| 基金项目： | 航空科学基金，江西省自然科学基金，江西省教育厅科研项目，南昌航空大学博上启动金 |
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| 摘 要： | 采用共沉淀法制备出性能良好的YAG(Y3A12(A1O4)3)纳米粉,对前驱体及不同温度下煅烧后的粉体进行差热、红外光谱、X射线衍射、比表面积和透射电镜等分析。结果表明:YAG粉体大小均匀,近似球形,且随着煅烧温度的升高,其颗粒逐渐变大,当温度达到1000℃时粉体全部为纯YAG立方相。随着母盐溶液(Y(NO3)3+Al(NO3)3)浓度的降低颗粒逐渐减少,并且粉体中YAM(Y4A12O9),Y2O3等相转化为纯YAG立方相。
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| 关 键 词： | 共沉淀法； YAG立方相； 煅烧温度； 母盐溶液浓度 |
Effect Factors of YAG Nano-Sized Powder by Co-precipitation Method |
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| LUO Jun-Ming and DENG Li-Ping. Effect Factors of YAG Nano-Sized Powder by Co-precipitation Method[J]. Chinese Journal of Inorganic Chemistry, 2010, 26(2): 240-244 |
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| Authors: | LUO Jun-Ming and DENG Li-Ping |
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| Affiliation: | School of Materials Science and Engineering, Nanchang Hangkong University, Nanchang 330063 and School of Materials Science and Engineering, Nanchang Hangkong University, Nanchang 330063 |
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| Abstract: | YAG nano-size powders were prepared by co-precipitation method, the precursor and powders after being calcined under different temperature were characterized by TG/DTA, IR, XRD, BET and TEM. The results show that YAG nano-size powders assumes spherically and distribute equably, and with the increase of calcination temperature, the grain increases gradually, the pure YAG cubic phase crystallite can be obtained at 1 000℃. With the decrease of mother solution concentration, the grain reduces gradually, and the YAM, Y_2O_3 phases of the powders change to pure YAG cubic phase. |
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| Keywords: | co-precipitation method YAG cubic phase calcination temperature mother solution concentration |
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