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Thermal behaviour of composites aluminosilicate-calcium phosphates
Authors:Derrien  A C.  Oudadesse  H.  Sangleboeuf  J. C.  Briard  P.  Lucas-Girot  A.
Affiliation:(1) Equipe Cristallochimie et Biomatériaux, Laboratoire CSIM UMR 6511 CNRS, Université de Rennes 1, Institut de Chimie de Rennes, Batiment 10b, Campus de Beaulieu 263 Av. Général Leclerc, C.S. 74205, 35042 Rennes, France E-mail;(2) Laboratoire LARMAUR UPRES JE 2310, Université de Rennes 1, Batiment 10b, Campus de Beaulieu 263 Av. Général Leclerc, C.S. 74205, 35042 Rennes, France
Abstract:A new type of aluminosilicate matrix calcium phosphate crystallites composites (ACPC) was synthesized and studied for osseous bone applications. The room temperature synthesis of the aluminosilicate matrix and composites was described. Thermal treatments of compounds allowed the adaptability of some parameters (pH, porosity and mechanical properties). Structure of heat treated composites were characterized by XRD and FTIR. The influence of thermal treatment on the mechanical properties, the porosity and the pH was studied for two temperatures (250 and 500°C). Results evidenced the ability to control the pH, the high level of porosity (»70%) and the good mechanical properties, allowing to consider that ACPC are potential biomaterials for osseous bone application.
Keywords:synthesis  thermal treatment  aluminosilicate  porosity  mechanical properties  mineral composition
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