Abstract: | In this study, TiO2 nanowires (TNWs) were synthesized through hydrothermal method and were characterized using X‐Ray diffraction (XRD), transmission electron microscopy (TEM) and BET techniques. Monoclinic TiO2 (B) is the dominant phase of TNWs up to 600°C which is completely transformed into a highly crystalline anatase phase at 800°C. The photocatalytic activity of TNWs, prepared at various calcination temperatures, was investigated in the removal of Rhodamine B as an organic model pollutant. The results indicated that the photocatalytic activity of TNWs, prepared at 800°C calcination temperature, was better than that of other samples and even TiO2–P25 nanoparticles. |