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Chromatographic packings made by solide phase synthesis
Authors:R. Ohmacht  Z. Matus
Affiliation:(1) University Madical School, P.O. Box 99, H-7643 Pécs, Hungary;(2) Labor Instrument Works, Esztergom, Hungary
Abstract:Summary A new way to produce liquid chromatographic stationary phases is suggested. The method is based upon a solide-phase reaction between the silica surface and the adsorbed silane molecules. The role of surface pH is demonstrated. The influence of other reaction conditions (concentration of the silane solution, effect of temperature and reaction time) is discussed.
Keywords:Column liquid chromatography  Synthesis of stationary phases  Influence of surface pH  Influence of temperature, concentration and reaction  time
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