| 软X射线分光晶体琥珀酸氢十四酯的合成及结晶习性研究 |
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| 引用本文： | 王桂美,高绍康,陈伟煌,林树坤. 软X射线分光晶体琥珀酸氢十四酯的合成及结晶习性研究[J]. 人工晶体学报, 2007, 36(6): 1412-1415 |
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| 作者姓名： | 王桂美 高绍康 陈伟煌 林树坤 |
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| 作者单位： | 福州大学化学化工学院,福州,350002;福州大学化学化工学院,福州,350002;福州大学化学化工学院,福州,350002;福州大学化学化工学院,福州,350002 |
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| 摘 要： | 本文合成了软X射线分光晶体琥珀酸氢十四酯(THS).通过红外光谱、差示量热扫描等手段对所合成样品进行表征和鉴定.对THS在苯、甲苯、二甲苯、异丙醇等溶剂中的自发成核和结晶形态进行了研究,结果表明THS在苯、甲苯和二甲苯中表现出良好的结晶习性.采用平衡法测定了THS在苯、甲苯和二甲苯中的溶解度曲线.综合考虑结晶习性和溶解度情况,可选择甲苯作为晶体生长的溶剂进行单晶生长实验.
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| 关 键 词： | 琥珀酸氢十四酯 分光晶体 结晶习性 溶解度 |
| 文章编号： | 1000-985X（2007）06-1412-04 |
| 收稿时间： | 2007-04-23 |
| 修稿时间： | 2007-04-23 |
Study on the Synthesis and Crystallinity of Tetradecyl Hydrogen Succinate Crystals for Soft X-ray Spectroscopy |
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| WANG Gui-mei,GAO Shao-kang,CHEN Wei-huang,LIN Shu-kun. Study on the Synthesis and Crystallinity of Tetradecyl Hydrogen Succinate Crystals for Soft X-ray Spectroscopy[J]. Journal of Synthetic Crystals, 2007, 36(6): 1412-1415 |
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| Authors: | WANG Gui-mei GAO Shao-kang CHEN Wei-huang LIN Shu-kun |
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| Abstract: | Tetradecyl hydrogen succinate(THS) was synthesized by esterification method.The sample of crystals was characterized by DSC,XRD and IR spectroscopy.The experiment results of crystallinity in some organic solvents showed that THS appears good crystal capability and habit in the benzene-liked solvents.The solubility curves of THS in these solvents were measured.Toluene was chosen as the solvent of THS crystals growth.The experiment of THS crystals growth are processing. |
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| Keywords: | tetradecyl hydrogen succinate analyzing crystal crystallinity solubility |
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