Interaction of dichloromethane with germanium |
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Authors: | V F Mironov T K Gar |
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Institution: | (1) N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences, USSR |
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Abstract: | Conclusions Methyltrichlorogermane, bis(trichlorogermyl)methane, and Ge-hexachloro-1,3,5-germacyclohexane are formed in good yield from dichloromethane and elementary germanium in a flow-type setup at 380°.Let us thank L. A. Leites for taking the IR and Raman spectra and A. N. Egorochkin for the NMR spectra.Translated from Izvestiya Akademii Nauk SSSR, Seria Khimicheskaya, No. 10, pp. 1887–1889, October, 1964 |
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