New representatives of nitroamine-containing 1,2,4-triazoles: Synthesis and structure |
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Authors: | T. P. Efimova O. Yu. Ozerova T. A. Novikova I. V. Belik V. M. Berestovitskaya |
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Affiliation: | 1. Herzen State Pedagogical University of Russia, Moyka emb. 48, St. Petersburg, 191186, Russia
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Abstract: | The interaction of 1-methyl-1-nitroso-2-nitroguanidine with carboxylic acid hydrazides results in formation of N-(2-nitroguanidino)amides that easily give 3(5)-nitroamino-5(3)-alkyl(aryl)-1,2,4-triazoles under refluxing in aqueous alkaline medium. We have developed a one-pot method to prepare such heterocyclic structures; the synthesis of one of the sample compound has given an example of the method applicability. The compounds structures have been confirmed by UV, IR, 1H, and 13C-{1H} NMR spectroscopy. |
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