Evaluation of the degree of hydration of tricalcium silicate pastes by quantitative differential thermal analysis |
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Authors: | Mascolo G |
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Institution: | (1) Istituto di Chimica Applicata, Facoltá d'Ingegneria della Universitá di Napoli, 80 125 Napoli, Italy |
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Abstract: | The hydration kinetics of C3S pastes can be easily evaluated by DTA using the most intense and reversible transition of C3S. Some modifications are proposed to Ramachandran's method concerning the measurement of this effect, the weight of the sample used for each experiment and the heating rate. The results of the hydration degree versus times of C3S agree reasonably with those reported by Ramachandran, while still better agreement is observed with those of Locher who used X-ray quantitative analysis.
Zusammenfassung Die Hydratisierungskinetik von C3S Pasten kann mittels DTA leicht bewertet werden, falls der intensivste und am meisten reversible Übergang von C3S genutzt wird. Einige Änderungen zur Methode von Ramachandran bezüglich der Messung dieses Effekts, des Gewichts der bei den einzelnen Messungen eingesetzten Proben und der Aufheizgeschwindigkeit werden vorgeschlagen. Die Ergebnisse des Hydratisierungsgrades von C3S in Abhängigkeit von der Zeit sind in guter Übereinstimmung mit denen von Ramachandran, während eine noch bessere Übereinstimmung mit den Werten von Locher beobachtet werden kann, welcher sich jedoch der quantitativen Röntgenanalyse bediente.
Résumé La cinétique de l'hydratation des pâtes de C3S peut être facilement déterminée par ATD, en utilisant la transition de C3S la plus intense, qui est réversible.On propose des modifications à la méthode de Ramachandran, concernant la mesure du phénomène, le poids des échantillons utilisés pour chaque expérience et le choix de la vitesse de chauffage. Les résultats donnant le degré d'hydratation de C3S en fonction du temps sont en bonne concordance avec ceux publiés par Ramachandran tandis qu'une concordance encore meilleure est observée avec les résultats de Locher obtenus par analyse quantitative aux rayons X.
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![icy](/content/x71570qt74u24567/xxlarge1080.gif) ![chcy](/content/x71570qt74u24567/xxlarge1095.gif) ![iecy](/content/x71570qt74u24567/xxlarge1077.gif) ![tcy](/content/x71570qt74u24567/xxlarge1090.gif) ![iecy](/content/x71570qt74u24567/xxlarge1077.gif) ![ncy](/content/x71570qt74u24567/xxlarge1085.gif) ![ncy](/content/x71570qt74u24567/xxlarge1085.gif) ![ycy](/content/x71570qt74u24567/xxlarge1099.gif) ![rcy](/content/x71570qt74u24567/xxlarge1088.gif) ![iecy](/content/x71570qt74u24567/xxlarge1077.gif) ![ncy](/content/x71570qt74u24567/xxlarge1085.gif) ![tcy](/content/x71570qt74u24567/xxlarge1090.gif) ![gcy](/content/x71570qt74u24567/xxlarge1075.gif) ![iecy](/content/x71570qt74u24567/xxlarge1077.gif) ![ncy](/content/x71570qt74u24567/xxlarge1085.gif) ![ocy](/content/x71570qt74u24567/xxlarge1086.gif) ![vcy](/content/x71570qt74u24567/xxlarge1074.gif) ![scy](/content/x71570qt74u24567/xxlarge1089.gif) ![kcy](/content/x71570qt74u24567/xxlarge1082.gif) ![acy](/content/x71570qt74u24567/xxlarge1072.gif) ![ncy](/content/x71570qt74u24567/xxlarge1085.gif) ![acy](/content/x71570qt74u24567/xxlarge1072.gif) ![lcy](/content/x71570qt74u24567/xxlarge1083.gif) ![icy](/content/x71570qt74u24567/xxlarge1080.gif) .
Financial support by Consiglio Nazionale delle Ricerche (Italy). |
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