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Development of novel synthetic method of carbon nanotubes from electrospun polystyrene fibers by using microwave heating
Authors:Tomohiro Ohta  Takeru Ito  Masahiro Shimizu  Lisa Tauchi  Huy‐Danh Nguyen‐Tran  Jong‐Chul Park  Byoung‐Suhk Kim  Ick‐Soo Kim  Kazuchika Ohta
Affiliation:1. Nano Fusion Technology Research Group, Department of Functional Machinery and Mechanics, Faculty of Textile Science and Technology, Shinshu University, Nagano 386‐8567, Japan;2. Smart Materials Science and Technology, Interdisciplinary Graduate School of Science and Technology, Shinshu University, Nagano 386‐8567, Japan
Abstract:We have developed a novel synthetic method that enables us to easily synthesize metal‐capsulated carbon nanotubes (CNTs) in a laboratory by using a combined technology of electrospinning‐metallization and microwave heating. These techniques greatly shorten the time for the synthesis of the CNTs in comparison with the conventional methods. TEM analysis confirmed a successful formation of the CNTs, and the resulting CNTs were multi‐walled and found to be about 25–100 nm in diameters. The products prepared by heating at 600 and 900°C exhibited less‐developed and strongly curved CNTs, whereas the products prepared by heating at 700 and 800°C relatively well‐developed long CNTs. Copyright © 2010 John Wiley & Sons, Ltd.
Keywords:carbon nanotubes  electrospinning  microwave heating
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