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Preparation of hollow carbon nanospheres at low temperature via new reaction route
Authors:Youbao Ni  Yanhua Tong  Guixiang Qian  Xianwen Wei
Affiliation:Auhui Key Laboratory of Functional Molecular Solids, College of Chemistry and Materials Science, Anhui Normal University, Number 1, Beijing East Road, Wuhu City, Anhui province 241000, P.R. China
Abstract:Hollow carbon nanospheres were obtained at 200 °C via a new reaction route, by using magnesium, hexachloroethane and aluminum trichloride as starting materials and benzene as solvent. The products were characterized with X-ray diffraction pattern, transmission electron microscope, high-resolution transmission electron microscope images and Raman spectrum. The reaction conditions are easy to be maintained and controlled. They may provide a new method to produce other carbonaceous materials. A possible mechanism of reaction was proposed.
Keywords:Nanostructure   Chemical synthesis   Grignard reagent   Hollow carbon nanospheres
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