Cubane Tellurido Clusters [Zn(NH3)4]3[Mo4Te4(CN)12] and [Cd(NH3)4]3[W4Te4(CN)12]: Syntheses and Crystal Structures |
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| Authors: | Kalinina I. V. Pervukhina N. V. Podberezskaya N. V. Fedin V. P. |
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| Affiliation: | (1) Siberian Division, Russian Academy of Sciences, Institute of Inorganic Chemistry, pr. Akademika Lavrent'eva 3, Novosibirsk, 630090, Russia |
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| Abstract: | Single crystals of [Zn(NH3)4]3[Mo4Te4(CN)12] (I) and [Cd(NH3)4]3[W4Te4(CN)12] (II) were obtained by applying solutions of K7[Mo4Te4(CN)12] · 11H2O and K6[W4Te4(CN)12] · 5H2O in aqueous ammonia over solutions of ZnCl2 and Cd(NO3)2 in glycerol and were characterized by X-ray diffraction analysis. The IR spectra and thermal properties of compounds I and II were examined. |
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