Obtaining
calcium carbonate in a multiphase system by the use of new rotating disc precipitation
reactor |
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Authors: | K K?dra-Królik P Gierycz |
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Institution: | (1) Institute of Physical Chemistry, Polish Academy of Sciences, Warszawa, Poland, 01-224, Kasprzaka 44/52 |
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Abstract: | Rotating disc reactor
(RDR) was constructed to conduct gas–liquid–solid reactions with
controlled reagent transfer from gaseous to liquid phase. The concept is based
on continuous formation of thin liquid films at a surface of rotating discs
where the mass transfer proceed in diffusion–convective way.
The reactor was employed
to run precipitation reaction of CaCO3 via carbon dioxide
absorption in lime slurry. During each reaction pH changes and Ca2+
concentration in time were measured. Disc rotations and gas flows were changed
during the experiment and their influence on the obtained CaCO3
powders has been examined and fully discussed. |
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Keywords: | calcium carbonate gas– liquid– solid reaction multiphase reactor precipitation |
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