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31P, 19F and 1H NMR spectroscopic study of the reaction of bis(trifluoromethyl)phosphine and solid KOH. Synthesis of the phosphaalkene CF3PCF2
Authors:Hossein E. Hosseini  Harold W. Kroto  John F. Nixon  Osamu Ohashi
Affiliation:School of Chemistry and Molecular Sciences, University of Sussex, Brighton BN1 9QJ, Sussex Great Britain
Abstract:The formation and subsequent reaction of the phosphaalkene CF3PCF2 obtained via dehydrofluorination of (CF3)2PH with KOH pellets at room temperature has been studied by multinuclear NMR spectroscopy.
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