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铂丝富集-火焰原子吸收光谱检测皮蛋中痕量铅
引用本文:黄燕. 铂丝富集-火焰原子吸收光谱检测皮蛋中痕量铅[J]. 分析测试技术与仪器, 2002, (3): 174-177.
作者姓名:黄燕
作者单位:1.岳阳师范学院化学化工系, 湖南, 岳阳, 414000
摘    要:一种运用火焰原子吸收测定皮蛋中铅含量的灵敏方法,它是通过用APDC-聚苯乙烯的化学方法修饰铂丝基质来实现的.预浓缩铅溶液后,将修饰的铂丝基质,放置在火焰燃烧器上,以便直接雾化并测定,在溶液中铅的浓度为5~500ng/mL范围内一般呈线性,检测的极限是0.65 ng/mL,这种方法既灵敏又方便.

关 键 词:火焰原子吸收  铂线圈  皮蛋  痕量铅
文章编号:1006-3757(2002)03-0174-04
收稿时间:2002-06-13
修稿时间:2002-06-13

Determination of Trace Lead in Preserved-egg by Flame Atomic Absorption Spectrometry
Huang Yan. Determination of Trace Lead in Preserved-egg by Flame Atomic Absorption Spectrometry[J]. Analysis and Testing Technology and Instruments, 2002, (3): 174-177.
Authors:Huang Yan
Affiliation:1.Department of Chemstry and Chemical Engineering, Yueyang Normal college, Yueyang 414000, China
Abstract:A sensitive method for the determination of lead in preserved egg by flame absorption spectrometry using ammonium pyrrolidine dithiocarbamate-polystyrene chemically modified platinum wire matrix is presented. The modifled platinum wire matrix, after preconcentrating the lead is placed in a flame burner for direct atomization and measurement. The concentration range is linear between 5 and ng/mL 500 ng/mL lead in solution and the detection limit is 0.65 ng/mL, this new technique is sensitive and convenient.
Keywords:flame atomic absorption  platinum wire coil  preserved-egg  trace lead
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