| 含氟内酯的核磁共振结构分析 |
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| 引用本文： | 史新梅,贺彩霞,周丽芳,潘铁英,邹小卫,吴范宏.含氟内酯的核磁共振结构分析[J].分析测试学报,2003,22(2):37-39. |
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| 作者姓名： | 史新梅 贺彩霞 周丽芳 潘铁英 邹小卫 吴范宏 |
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| 作者单位： | 1. 华东理工大学,分析测试中心,上海,200237
2. 华东理工大学,精细化工研究所,上海,200237 |
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| 摘 要： | 利用核磁共振中^1H、^13C和^19F谱以及二维技术对含氟内酯的结构及空间构型进行了研究，并对全部谱峰进行了归属，为含氟内酯合成反应的顺利进行提供了理论依据。
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| 关 键 词： | 含氟内酯 核磁共振 化学位移 |
| 文章编号： | 1004-4957(2003)02-0037-03 |
| 修稿时间： | 2002年4月26日 |
NMR Studies on Fluorine-containing Lactones |
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| SHI Xin-mei ,HE Cai-xia ,ZHOULi-fang ,PAN Tie-ying ,ZHOUXiao-wei ,WUFan-hong.NMR Studies on Fluorine-containing Lactones[J].Journal of Instrumental Analysis,2003,22(2):37-39. |
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| Authors: | SHI Xin-mei HE Cai-xia ZHOULi-fang PAN Tie-ying ZHOUXiao-wei WUFan-hong |
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| Institution: | SHI Xin-mei 1,HE Cai-xia 1,ZHOULi-fang 1,PAN Tie-ying 1,ZHOUXiao-wei 2,WUFan-hong 2 |
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| Abstract: | Fluorine-containing lactones were studied by nuclear magnetic resonance spectroscopy.The structure and configuration of two fluorine - containing lactones were determined by 1 H NMR, 13 C NMR, 1 H- 1 H COSY,NOESY,HMQC and HMBC. 19 F NMR was also used for determining halogen- and fluorine-containing alkyl in the samples.This method is useful for the research of synthetic reaction. |
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| Keywords: | Fluorine-containing lactones NMR Chemical shifts |
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