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溶胶-凝胶法研制中空玻璃珠
引用本文:周梅芳,周赛玉,王妍. 溶胶-凝胶法研制中空玻璃珠[J]. 华东理工大学学报(自然科学版), 1992, 0(Z1)
作者姓名:周梅芳  周赛玉  王妍
作者单位:华东化工学院无机材料系,华东化工学院无机材料系,华东化工学院无机材料系
摘    要:选择溶胶-凝胶粉末静态成珠法,制得了(Li_2O)-Na_2O-B_2O_3-SiO_2系统中空玻璃珠。用红外吸收光谱研究了凝胶结构随热处理温度的变化。随温度升高,Si—O—C_2H_5、Si—OH键逐渐消失,而Si—O—B,B—O,Si—O键逐渐形成和增加。借助光学显微镜、扫描电子显微镜观察了玻璃珠的中空状态和表面形貌。并探讨了成珠方法、过程及珠密度的影响因素。

关 键 词:溶胶-凝胶法  结构分析  密度  Na_2O-B_2O_3-SiO_2凝胶  中空玻璃珠

Preparation of Hollow Glass Sphere by Sol-Gel Method
Zhou Meifang,Zhou Saiyu Wan Yan. Preparation of Hollow Glass Sphere by Sol-Gel Method[J]. Journal of East China University of Science and Technology, 1992, 0(Z1)
Authors:Zhou Meifang  Zhou Saiyu Wan Yan
Affiliation:Department of Inorganic Materials
Abstract:The hollow glass sphere in Na_2O-B_2O_3-SiO_2 system was prepared at static state by gel powder via sol-gel process. Its structure was studied by IR spectra. The hollow state and surface morphology of glass sphere was observed by SEM and optical microscope. The form method, process and the effects of various factors on density of hollow glass sphere were discussed.
Keywords:sol-gel process  structural analysis  density  Na_2O-B_2O_3-SiO_2 system  hollowglass sphere
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