Synthesis of 1,2,3,4-tetrazino[5,6-g]benzo-1,2,3,4-tetrazine 1,3,7,9-tetraoxides |
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Authors: | A E Frumkin A M Churakov Yu A Strelenko V A Tartakovsky |
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Institution: | (1) N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 119991 Moscow, Russian Federation |
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Abstract: | 1,2,3,4-Tetrazino5,6-g]benzo-1,2,3,4-tetrazine 1,3,7,9-tetraoxides, which possess an-thracene-type annulation of the benzene ring with two 1,2,3,4-tetrazine
1,3-dioxide fragments, were obtained for the first time from aminobenzenes containing tert-butyl-NNO-azoxy groups in appropriate positions. Complete assignments of the signals in the 1H, 13C, and 14N NMR spectra of the compounds obtained were carried out.
Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 9, pp. 1595–1599, September, 2006. |
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Keywords: | benzo-1 2 3 4-tetrazines N-oxides N-nitroamines azoxy compounds 13C NMR spectroscopy |
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