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Synthesis and X-Ray Crystal Structure Study of ]2-Methyl-4-(2-methylbenzoyl)-phenoxy] Acetic Acid Hydrazide
Authors:Mahendra  Madegowda  Doreswamy  Beeranahally H.  Sridhar  Mandayam A.  Prasad  Javaregowda S.  Khanum  Shaukath A.  Shashikanth  Sheena  Sudha  Belagur S.
Affiliation:(1) Department of Studies in Physics, University of Mysore, Manasagangotri, Mysore, 570 006, India;(2) Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore, 570 006, India
Abstract:Benzophenone analog 3 has been synthesized and characterized by the X-ray diffraction (XRD) method. The compound crystallizes in a monoclinic space group P21/c with cell parameters a = 7.701(8) Å, b = 7.151(5) Å, c= 28.323(3) Å, beta = 104.639(4)°, Z = 4. The structure exhibits intra- and intermolecular hydrogen bonding of the type N–HsdotsdotsdotO, C–HsdotsdotsdotO, and N–HsdotsdotsdotN. The molecules are interlinked through hydrogen bonds forming an infinite chain. This polymeric-like structure may play an important role in biological activity.
Keywords:Benzophenone analog  polymeric structures  C–  H  /content/hk1675u9m65164v2/xxlarge8901.gif"   alt="  sdot"   align="  BASELINE"   BORDER="  0"  >  /content/hk1675u9m65164v2/xxlarge8901.gif"   alt="  sdot"   align="  BASELINE"   BORDER="  0"  >  /content/hk1675u9m65164v2/xxlarge8901.gif"   alt="  sdot"   align="  BASELINE"   BORDER="  0"  >O hydrogen bonds
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