| 对氟苯甲醛水杨酰腙镍(II)配合物的合成、表征及其晶体结构 |
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| 引用本文： | 张淑萍,刘昭第,陈水生,魏影,邵思常. 对氟苯甲醛水杨酰腙镍(II)配合物的合成、表征及其晶体结构[J]. 无机化学学报, 2007, 23(6): 1069-1071 |
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| 作者姓名： | 张淑萍 刘昭第 陈水生 魏影 邵思常 |
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| 作者单位： | 阜阳师范学院化学系,阜阳,236041 |
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| 基金项目： | 安徽省高校自然科学资金项目 |
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| 摘 要： | A nickel(II) complex Ni(C14H10N2O2F)2 was synthesized from p-fluorobenzaldehyde salicylhydrazone and Ni(CH3COO)2·4H2O and crystallized by diffusion, the structure of which was characterized by IR spectrum, 1H NMR, and X-ray single-crystal diffraction. The complex crystallizes in monoclinic space group C2/c with a=2.460 6(2) nm, b=0.774 1(1) nm, c=1.534 9(1) nm, β=122.300(1)°, and V=2.471 1(4), Z=8, Dc=1.541 g·cm-3. We reported the IR, 1H NMR, crystal structure. CCDC: 638652.
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| 关 键 词： | 对氟苯甲醛水杨酰腙； 镍配合物； 晶体结构； 合成 |
| 文章编号： | 1001-4861（2007）06-1069-03 |
| 修稿时间： | 2006-11-272007-02-27 |
Synthesis, Characterization and Crystal Structure of Bis(p-fluorobenzaldehyde salicylhydrazone) Nickel(II) |
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| ZHANG Shu-Ping,LIU Zhao-Di,CHEN Shui-Sheng,WEI Ying and SHAO Si-Chang. Synthesis, Characterization and Crystal Structure of Bis(p-fluorobenzaldehyde salicylhydrazone) Nickel(II)[J]. Chinese Journal of Inorganic Chemistry, 2007, 23(6): 1069-1071 |
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| Authors: | ZHANG Shu-Ping LIU Zhao-Di CHEN Shui-Sheng WEI Ying SHAO Si-Chang |
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| Affiliation: | Department of Chemistry, Fuyang Normal College, Fuyang, Anhui 236041,Department of Chemistry, Fuyang Normal College, Fuyang, Anhui 236041,Department of Chemistry, Fuyang Normal College, Fuyang, Anhui 236041,Department of Chemistry, Fuyang Normal College, Fuyang, Anhui 236041 and Department of Chemistry, Fuyang Normal College, Fuyang, Anhui 236041 |
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| Abstract: | |
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| Keywords: | p-fluorobenzaldehyde salicylhydrazone nickel(II) complex crystal structure synthesis |
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