Thermoanalytical studies of the kinetic of reversible reactions |
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Authors: | N I Vaganova V I Rozenband V V Barzykin |
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Institution: | (1) Department of the Institute of Chemical Physics, Academy of Sciences of the U.S.S.R., Chernogolovka, U.S.S.R. |
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Abstract: | A method is described for determination of the kinetic parameters of reversible reactions under isothermal and non-isothermal conditions in thermal analysis. Reversible reactions of the first and second orders and of mixed types are considered. The kinetic parameters of the forward and reverse reactions are determined on the basis of the initial integral data of the thermoanalytical experiment. The results of processing a computerized experiment demonstrated that the suggested method is satisfactorily applicable.
Zusammenfassung Es wurde eine Methode zur Bestimmung kinetischer Parameter von reversiblen Reaktionen unter isothermen bzw. nicht-isothermen Umständen in der Thermoanalyse beschrieben. Umkehrbare Reaktionen erster Ordnung, zweiter Ordnung sowie Reaktionen vom Mischtyp wurden betrachtet. Die kinetischen Parameter der Hin- bzw. Rückreaktionen wurden auf der Grundlage der Anfangsintegrale der termoanalytischen Experimente bestimmt. Die Ergebnisse eines computermodellierten Experimentes zeigen, dass die vorgeschlagene Methode befriedigend angewendet werden kann.
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![gcy](/content/u88306750h1um854/xxlarge1075.gif) ![mcy](/content/u88306750h1um854/xxlarge1084.gif) ![iecy](/content/u88306750h1um854/xxlarge1077.gif) ![tcy](/content/u88306750h1um854/xxlarge1090.gif) ![ocy](/content/u88306750h1um854/xxlarge1086.gif) .
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