| Synthesis of A Novel Fulleroaziridine Carrying 4-Deoxy-4＇-demethylepipodophyllotoxin |
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| 作者姓名： | QianRongLI ShaYANG |
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| 作者单位： | StructureResearchLaboratory,UniversityofScienceandTechnologyofChina,Hefei230026 |
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| 摘 要： | A novel fulleroaziridine 2 with a closed 6,6-ring junction was synthesized from 60]fullerene and 4-azido-4-deoxy- 4‘-demethylepipodophyllotoxin 1 in 1, 2-dichlorobenzene at 110℃ for 45 h, in a yield of 39.3 % based on consumed C60. The structure of the product was characterized by NMR and MS.
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| 关 键 词： | 合成 球壳状氮丙啶 4-脱氧-4＇-脱甲基表足叶草毒素 足叶草毒素衍生物 叠氮化物 环加成反应 C60 1 2-二氯苯 |
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