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原子荧光光谱法测定杜仲中的砷
引用本文:朱琳,曾晓丹,张福胜. 原子荧光光谱法测定杜仲中的砷[J]. 光谱实验室, 2012, 29(2): 973-976
作者姓名:朱琳  曾晓丹  张福胜
作者单位:吉林化工学院化学与制药工程学院,吉林省吉林市龙潭区承德街45号,132022
基金项目:吉林化工学院科研基金资助项目
摘    要:采用双通道原子荧光光谱法测定杜仲中砷的含量。确定了仪器的最佳工作条件,考察了酸度、还原剂、预还原剂的影响以及共存元素的干扰情况。方法快速、简便、准确且灵敏度高,为中药材中砷的含量测定提供了较好的方法。

关 键 词:原子荧光光谱法  杜仲  

Determination of Arsenic in Eucommia by Atomic Fluorescence Spectrometry
ZHU Lin , ZENG Xiao-Dan , ZHANG Fu-Sheng. Determination of Arsenic in Eucommia by Atomic Fluorescence Spectrometry[J]. Chinese Journal of Spectroscopy Laboratory, 2012, 29(2): 973-976
Authors:ZHU Lin    ZENG Xiao-Dan    ZHANG Fu-Sheng
Affiliation:ZHU Lin ZENG Xiao-Dan ZHANG Fu-Sheng(School of Chemical and Pharmaceutical Engineering,Jilin Institute of Chemical Technology,Jilin,Jilin 132022,P.R.China)
Abstract:The content of arsenic in eucommia was determined by hydride generation-atomic fluorescence spectrometry.The optimal conditions were established,and the influence factors such as the acidity,the concentration of reducer and prereducer,and the interference of co-exiting elements were discussed.This method is proved to be fast,simple,accurate and sensitive,and it offers a good metod for the determination of arsenic in traditional Chinese medicine.
Keywords:Atomic Fluorescence Spectrometry  Eucommia  Arsenic  Inorganic Arsenic
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