| 胃复宁片的质量标准 |
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| 引用本文： | 罗国平,孟会宁,赵宁. 胃复宁片的质量标准[J]. 光谱实验室, 2012, 29(2): 702-706 |
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| 作者姓名： | 罗国平 孟会宁 赵宁 |
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| 作者单位： | 1. 西安医学院药学院,西安市辛王路1号,710021
2. 西安步长医药有限公司,西安市高新区高新路,710075 |
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| 基金项目： | 2010年陕西省教育厅专项科研计划项目(2010JK812),2011年陕西省教育厅专项科研计划项目(11JK0696) |
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| 摘 要： | 建立胃复宁片的质量标准。采用薄层色谱法对胃复宁片中的延胡索和白术进行鉴别;采用HPLC测定胃复宁片中延胡索乙素的含量。薄层色谱斑点清晰,阴性对照无干扰;延胡索乙素含量在0.22—1.10μg范围内与峰面积呈良好线性关系(r=0.9992);平均回收率为97.1%,RSD=2.09%(n=6)。方法简单、准确、重现性好,可有效地控制胃复宁片的质量。
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| 关 键 词： | 胃复宁片 延胡索乙素 薄层色谱 高效液相色谱法 |
Quality Standard of Weifuning Tablets |
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| Luo Guo-Ping , MENG Hui-Ning , ZHAO Ning. Quality Standard of Weifuning Tablets[J]. Chinese Journal of Spectroscopy Laboratory, 2012, 29(2): 702-706 |
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| Authors: | Luo Guo-Ping MENG Hui-Ning ZHAO Ning |
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| Affiliation: | LUO Guo-Ping MENG Hui-Ninga ZHAO Ning(School of Pharmacy,Xi’an Medical University,Xi’an 710021,P.R.China)a(Xi’an Buchang Medicine Limited Company,Xi’an 710075,P.R.China) |
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| Abstract: | Quality standard of Weifuning tablets was established.Corydalis tuber and bighead atractylodes rhizome were identified by thin layer chromatography(TLC),while the content of tetrahydropalmatine was determined by high performance liquid chromatography(HPLC).The results showed that the TLC sports developed were fairly clear,and the blank test showed no interference.The peak area has a good linear relationship with the content of tetrahydropalmatine in the range of 0.22—1.10μg(r=0.9992).The average recovery was 97.1% with RSD of 2.09%(n=6).The method proved to be simple,accurate and reproducible.The quality standard can effectively control the quality of Weifuning tablets. |
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| Keywords: | Weifuning Tablets Tetrahydropalmatine TLC HPLC |
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