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微波消解吸载乙醇活性炭出口浓度的近似法测定
引用本文:连明磊,冯权莉,宁平,胡江良,李志.微波消解吸载乙醇活性炭出口浓度的近似法测定[J].光谱实验室,2012,29(3):1615-1619.
作者姓名:连明磊  冯权莉  宁平  胡江良  李志
作者单位:1. 六盘水师范学院环境与化学工程系 贵州省六盘永市钟山区明湖路育才巷19号 553004
2. 昆明理工大学化学工程学院 昆明市650224
3. 昆明理工大学环境科学与工程学院 昆明市 650093
基金项目:云南省教育厅科学研究基金项目,六盘水市科技计划项目
摘    要:设计了载乙醇活性炭微波解吸的实验流程。采用近似法测定载乙醇活性炭微波解吸的出口浓度曲线,对微波解吸的分离过程进行了分析。实验结果表明,中期乙醇出口浓度高于前后期;在320W微波功率下,90s即出现乙醇出口浓度的最高峰值;在680W微波功率下,60s即出现乙醇出口浓度的最高峰值;质量分数4%的低浓度乙醇水溶液经两次活性炭吸附-微波解吸循环后,乙醇出口质量分数的峰值可达94%以上。

关 键 词:微波解吸  气相色谱  近似法  乙醇

Approximation Determination of Outlet Concentration of Microwave Desorbed Ethanol-Loaded Activated Carbon
LIAN Ming-Lei , FENG Quan-Li , NING Ping , HU Jiang-Liang , LI Zhi.Approximation Determination of Outlet Concentration of Microwave Desorbed Ethanol-Loaded Activated Carbon[J].Chinese Journal of Spectroscopy Laboratory,2012,29(3):1615-1619.
Authors:LIAN Ming-Lei  FENG Quan-Li  NING Ping  HU Jiang-Liang  LI Zhi
Institution:LIAN Ming-Lei FENG Quan-Li a NING Ping b HU Jiang-Liang LI Zhi(Department of Environmental and Chemical Engineering,Liupanshui Normal College,Liupanshui,Guizhou 553004,P.R.China)a(Faculty of Chemical Engineering,Kunming University of Science and Technology,Kunming 650224,RP.China)b(Faculty of Environmental Science and Engineering,Kunming University of Science and Technology,Kunming 650093,P.R.China)
Abstract:The experiment process for microwave desorption of ethanol-loaded activated carbon was designed.The outlet concentration curves of microwave desorbed ethanol-loaded activated carbon were determined by approximation method,and the separation processes of the microwave desorption was analyzed.The experimental results showed that the medium-term outlet concentration was higher than former and later term.The highest value appeared at 90s when the microwave power was 320W,and at 60s when the microwave power was 680W.After the ethanol mass fraction of 4% was cycled by two times processes of activated carbon adsorption and microwave desorption,the mass fraction of ethanol can come up to more than 94%.
Keywords:Microwave Desorption  Gas Chromatogram  Approximation  Ethanol
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