| N-丁基-3,6-二乙酰基咔唑的合成及表征 |
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| 引用本文： | 董金龙,张永斌,张改玲,张丽.N-丁基-3,6-二乙酰基咔唑的合成及表征[J].光谱实验室,2012,29(3):1827-1829. |
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| 作者姓名： | 董金龙 张永斌 张改玲 张丽 |
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| 作者单位： | 1. 太原师范学院化学系 太原市黄陵路19号 030031
2. 山西大学化学化工学院 太原市坞城路92号 030006 |
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| 基金项目： | 2011年度山西省高校科技开发项目 |
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| 摘 要： | 以咔唑为合成原料,在相转移催化剂作用下合成N-丁基咔唑,作为电子给体和共轭桥中心,乙酰氯作为端基电子受体,合成了V型化合物:N-丁基3,6-二乙酰基咔唑。其结构经IR,1H NMR和GC-MS表征。
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| 关 键 词： | 咔唑 合成 表征 |
Synthesis and Characterization of N-Butyl-3,6-Diacetyl Carbazole |
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| DONG Jin-Long
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ZHANG Yong-Bin
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ZHANG Gai-Ling
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ZHANG Li.Synthesis and Characterization of N-Butyl-3,6-Diacetyl Carbazole[J].Chinese Journal of Spectroscopy Laboratory,2012,29(3):1827-1829. |
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| Authors: | DONG Jin-Long ZHANG Yong-Bin ZHANG Gai-Ling ZHANG Li |
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| Institution: | DONG Jin-Long ZHANG Yong-Bin a ZHANG Gai-Ling ZHANG Li(Department of Chemistry,Taiyuan Normal University,Taiyuan 030031,P.R.China)a(School of Chemistry and Chemical Engineering,Shanxi University,Taiyuan 030006,P.R.China) |
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| Abstract: | N-butyl-carbazole that was as electron donor and conjugate bridge center,was prepared under the phase transfer catalyst effect with carbazole as composition raw meterial and acetylchloride as the end group electronic receptor.Base on the conditions,the V-type compounds,N-butyl-3,6-diacetyl carbazole,were synthesized.The structures of the compounds were charecterized by IR,1H NMR and GC-MS. |
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| Keywords: | Carbazole Synthesis Characterization |
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