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| N-苯基和N-乙氧羰基甲基磷异喹啉酮及其衍生物的合成 | |
| 引用本文： | 丁一,丁贻祥.N-苯基和N-乙氧羰基甲基磷异喹啉酮及其衍生物的合成[J].有机化学,2008,28(10):1744-1749. |
| 作者姓名： | 丁一 丁贻祥 |
| 作者单位： | 1. 上海师范大学牛命与环境科学学院,上海,200234 2. 中国科学院上海有机化学研究所,上海,200032 |
| 摘 要： | 以邻炔基苯磷酰胺为原料经Pd(II)催化的环化反应、环化偶联反应和氯环化反应高收率合成了15个N-苯基和N-乙氧羰基甲基磷异喹啉酮及其4-烯丙基、4-氯衍生物, 它们的结构均经过1H NMR, 13C NMR, MS, IR及元素分析确证. |
| 关 键 词： | N-苯基磷异喹啉酮 N-乙氧羰基甲基磷异喹啉酮 环化 环化偶联 氯环化 4-取代磷异喹啉酮 |
| 收稿时间： | 2008-3-17 |
| 修稿时间： | 2008-4-28 |
Synthesis of N-Phenyl and N-Ethoxycarbonylmethyl Phosphaisoqui-nolin-1-ones and Their Derivatives |
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| DING,Yi,DING,Yi-Xian.Synthesis of N-Phenyl and N-Ethoxycarbonylmethyl Phosphaisoqui-nolin-1-ones and Their Derivatives[J].Chinese Journal of Organic Chemistry,2008,28(10):1744-1749. | |
| Authors: | DING Yi DING Yi-Xian |
| Institution: | (a College of Life and Environment Sciences, Shanghai Normal University, Shanghai 200234) (b Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032) |
| Abstract: | Fifteen N-phenyl and N-ethoxycarbonylmethyl phosphaisoquinolin-1-ones and their 4-allyl, 4-chloro derivatives were synthesized by Pd(II)-catalyzed cyclization, coupling-cyclization and halocyclization reactions. The structures of the target compounds were confirmed by 1H NMR, 13C NMR, MS, IR spectra and elemental analysis. |
| Keywords: | N-phenyphosphaisoquinolin-1-one N-ethyloxygencarbonylmethylphosphaisoquinolin-1-one cyclization coupling-cyclization halocyclization 4-substituent phosphaisoquinolin-1-one |
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