Complete 1H and 13C NMR spectral assignment of 17-hydroxy epimeric sterols with planar A or A and B rings |
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| Authors: | Ciuffreda P Casati S Manzocchi A |
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| Institution: | Dipartimento di Scienze Precliniche LITA Vialba, Università di Milano, Via G. B. Grassi 74, 20157 Milan, Italy. |
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| Abstract: | Complete 1H and 13C spectral assignments of 17beta- and 17alpha-hydroxy epimers of three biologically active sterols (boldenone, 3-methoxyestradiol and 3-methoxydihydroequilenin) were achieved making use of one- and two-dimensional NMR techniques (1D-HOHAHA, DEPT, COSY, NOESY, TOCSY, HSQC and COLOC). |
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| Keywords: | NMR 1H NMR 13C NMR 1D‐HOHAHA COSY NOESY TOCSY HSQC COLOC sterols 17β‐ and 17α‐hydroxy epimers |
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