| 气敏材料Cd2V2O7的制备和性能 |
| |
| 引用本文： | 赖琼钰,卢集政.气敏材料Cd2V2O7的制备和性能[J].应用化学,1999,16(2):56-59. |
| |
| 作者姓名： | 赖琼钰 卢集政 |
| |
| 作者单位： | 四川大学化学学院 |
| |
| 摘 要： | 用水热氧化法制备出γＭｎ２Ｏ３粉末，并在不同温度下进行烧结．采用ＸＲＤ，ＴＥＭ，ＸＰＳ，ＩＲ及紫外分光光度法等表征产物．结果表明，未烧结产物即为单相纳米晶，大部分近似球形，有轻微团聚．产物于空气中１００～５５０℃范围内烧结时热稳定性好．随烧结温度的升高粉末的平均粒子尺寸增大，产物中锰以Ｍｎ（Ⅲ）状态存在．
|
| 关 键 词： | γ-Mn_2O_3，纳米粉末，制备，水热氧化 |
Preparation of Mn2O3 by Oxidation Under Hydrothermal Conditions |
| |
| Lai Qiongyu,Lu Jizheng,Xiao Shuxing,Zheng Zonghe.Preparation of Mn2O3 by Oxidation Under Hydrothermal Conditions[J].Chinese Journal of Applied Chemistry,1999,16(2):56-59. |
| |
| Authors: | Lai Qiongyu Lu Jizheng Xiao Shuxing Zheng Zonghe |
| |
| Institution: | Lai Qiongyu*,Lu Jizheng,Xiao Shuxing,Zheng Zonghe |
| |
| Abstract: | Ultrafine Mn2O3 powder was prepared by an oxidation method under hydrothermal conditions. After sintering at 100550 in air the products exhibit good stability and have been characterized by XRD, TEM, XPS, IR and UV spectra measurements to be fine crystals of single phase, majority in ball form. Their average sizes increase with increase of the sintering temperatures. The manganese in Mn2O3 is in Mn() form. |
| |
| Keywords: | Mn2O3 nanometer powder preparation hydrothermal oxidation |
| 本文献已被 CNKI 维普 等数据库收录！ |
| 点击此处可从《应用化学》浏览原始摘要信息 |
| 点击此处可从《应用化学》下载免费的PDF全文 |
|
