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Structural and vibrational studies of anilinium nitrate
Authors:MK Marchewka  A Pietraszko
Institution:Institute of Low Temperature and Structure Research, Polish Academy of Sciences, P.O. Box 937, 50-950 Wroc?aw 2, Poland
Abstract:The crystals of anilinium nitrate, View the MathML source, were obtained by slow evaporation of an aqueous solution. The crystals belong to the Pbca (no. 61) space group of orthorhombic system, Z=8, a=10.158(2), b=9.277(2), c=16.177(3) Å. Positively charged anilinium cations and View the MathML source anions are present in the structure. Powder FT IR and FT Raman spectra for normal and deuterated samples are discussed with respect to the crystal structure. DSC measurements do not indicate clearly on the occurrence of phase transition in the temperature region 113-293 K.
Keywords:C  Infrared spectroscopy  C  Raman spectroscopy  D  Crystal structure
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