Inhibition kinetic determination of trace amount of iodide by the spectrophotometric method with rhodamine B |
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Authors: | Zhu Xiashi Zhang Yiaqin |
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Institution: | Department of Chemistry, Yangzhou University, Yangzhou 225002, PR China. xszhu@yzu.edu.cn |
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Abstract: | Trace iodide was determined by inhibition kinetic method, which based on its inhibition effects on the reaction between rhodamine B (RhB) and KBrO(3) in H(2)SO(4) medium in 45+/-0.5 degrees C for 15 min. The signal difference (DeltaA, DeltaF) between inhibited reaction and non-inhibited reaction is linear with the concentration of iodide. The linear range were 2.0-6.0 and 1.0-6.0 ng mL(-1) and the detection limit were 0.06 and 0.07 ng mL(-1), respectively. The method has been applied satisfactorily to the determination of iodide in kelp. |
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