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| 原子吸收光谱法测定中成药中微量元素 | |
| 引用本文： | 孙瑞霞,周玲妹,薛万刚,孙剑辉. 原子吸收光谱法测定中成药中微量元素[J]. 光谱学与光谱分析, 2002, 22(5): 853-855 |
| 作者姓名： | 孙瑞霞 周玲妹 薛万刚 孙剑辉 |
| 作者单位： | 1. 河南师范大学化学与环境科学学院,河南省高等学校环境科学与工程重点实验室,河南,新乡,453002 2. 河南农业大学基础科学学院,河南,郑州,450002 3. 新乡市红旗医院,河南,新乡,453000 |
| 基金项目： | 河南省自然科学基金资助项目 (No 1 9991 50 0 30 ) |
| 摘 要： | 采用HNO3－HClO4(4:1)混酸消化用于治疗糖尿病的消渴丸、玉泉丸、渴乐宁、降糖舒、降糖Ⅰ-Ⅴ号9种中成药，用原子吸收光谱法对药物消化液中的Cu,Zn,Ni,Co,Mn,Cr,Mo,Fe,Ca,Mg,Cd,Pb12种微量元素进行了分析测定。该方法的加标回收率为97％－105％，相对标准偏差（RSD）小于5％，具有良好的准确度和精密度。结果表明：糖尿病类中成药中除Cd,Pb外，其余10种元素的含量均较为丰富，本测定结果为探讨上述糖尿病类中成药中微量元素的含量与药效的相关关系提供了有用的数据。 |
| 关 键 词： | 测定 原子吸收光谱法 糖尿病 中成药 微量元素 药效 分析 |
| 文章编号： | 1000-0593(2002)05-0853-03 |
| 修稿时间： | 2001-12-20 |
Determination of Trace Elements in Chinese Traditional Medicines by Atomic Absorption Spectrometry |
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| SUN Rui-xia ,ZHOU Ling-mei ,XUE Wan-gang ,and SUN Jian-hui .Chemistry and Environmental Sciences College of Henan Normal University,Environmental Sciences and Engineering Key Open Laboratory of Henan Colleges and Universities,Xinxiang. Determination of Trace Elements in Chinese Traditional Medicines by Atomic Absorption Spectrometry[J]. Spectroscopy and Spectral Analysis, 2002, 22(5): 853-855 | |
| Authors: | SUN Rui-xia ZHOU Ling-mei XUE Wan-gang and SUN Jian-hui .Chemistry Environmental Sciences College of Henan Normal University Environmental Sciences Engineering Key Open Laboratory of Henan Colleges Universities Xinxiang |
| Affiliation: | Chemistry and Environmental Sciences, College of Henan Normal University, Environmental Sciences and Engineering, Key Open Laboratory, Henan Colleges and Universities, Xinxiang 453002, China. |
| Abstract: | The 9 kinds of Chinese traditional medicines which are used to cure diabetes including Xiaokewan, Yuquanwan, Kelening, Jiangtangshu, Jiangtang I-V are digested with HNO3-HClO4 (4:1) mixed acid. The 12 trace elements of copper, zinc, nickel, cobalt, manganese, chromium, molybdenum, iron, calcium, magnesium, cadmium and lead in the solution are determined by atomic absorption spectrometry. Its recovery ratio by standard addition is 97%-105%, and RSD is lower than 5%. This method has good accurate. The results obtained show that except Cd and Pb all other ten trace elements contents in the drug are high. The results of this paper provide useful data for studying the relation between the contents of these trace elements and the medical effect. |
| Keywords: | Atomic absorption spectrometry Diabetes Chinese traditional medicines Trace elements |
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