Preconcentration of phenols by adsorption on organo-clay followed by capillary electrophoretic determination |
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Authors: | F B Erim and I Alemdar |
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Institution: | (1) Department of Chemistry, Technical University of Istanbul, Maslak, 80626, Istanbul, Turkey, TR |
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Abstract: | The organo-clay adsorbent used was prepared by modification of montmorillonite from Kurşunlu, Turkey with the cationic surfactant
cetyltrimethlyammonium bromide. The modification process involves replacing the inorganic exchange cations of the clay by
organic cations containing long chain alkyl groups. The retention of phenolic compounds from aqueous solution on the organo-clay
was studied. The analytes are quantitatively retained on the proposed adsorbent at pH 7 and recovered by elution with ethanol.
The determination of phenols was performed by capillary electrophoresis.
Received: 28 July 1997 / Revised: 15 December 1997 / Accepted: 8 January 1998 |
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