Recent progress in numerical methods for the determination of thermokinetics |
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Authors: | E. Cesari P. C. Gravelle J. Gutenbaum J. Hatt J. Navarro J. L. Petit R. Point V. Torra E. Utzig W. Zielenkiewicz |
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Affiliation: | (1) Facultad de Fisica, Departamento de Terminologia, Barcelona-28, Spain;(2) Institut de Recherches sur la Catalyse, CNRS, 69626 Villeurbanne, France;(3) System Research Institute, PAN, 01-447 Warszawa, Poland;(4) Institute of Physical Chemistry, PAN, 01-224 Warszawa, Poland;(5) Departamento de Fisica, ETSEIB, Barcelona-28, Spain;(6) Dept. d'Automatique et Dynamique des Systemes, Université Aix- Marseille III, 13397 Marseille, France;(7) Dept. d'Informatique, INSA, 69621 Villeurbanne, France |
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Abstract: | The results of a multinational concerted programme on the determination of thermokinetics are presented. The purpose of the programme was to compare different numerical methods which have been independently proposed for the determination of thermokinetics from experimental calorimetric data. To achieve this end, the same experimental data, obtained from two heat-flow calorimeters, were distributed and successively analyzed by the different methods. Numerical methods based on the state function theory, on Fourier transform analysis, on dynamic optimization and on a simple differentiation of the data were thus critically tested.
Zusammenfassung Es wurden die Ergebnisse der gemeinsamen Arbeiten über die Bestimmung der Thermokinetik mit 4 numerischen Methoden (dynamische Optimalisierung, Methode der Zustandfunktionen, harmonische Analyse und umgekehrte Korrektion) vorgestellt. Die experimentellen Daten wurden mit Hilfe von 2 Kalorimetern mit einer konstanten Temperatur des Isoliermantels ermittelt. Die Durchführung der Versuche ermöglichte ein Vergleich der angewandten Methoden.
Résumé Les résultats d'un programme de recherches concerté multinational sur la détermination des données thermocinétiques sont présentés. Le but du programme était de comparer différentes méthodes numériques proposées indépendamment pour la détermination des données thermocinétiques à partir des mesures calorimétriques expérimentales. Pour celà, les mêmes données expérimentales fournies par deux calorimètres à flux de chaleur ont été distribué es et analysées successivement par 4 méthodes: utilisation des variables d'état, analyse de la transformée de Fourier, optimalisation dynamique et simple différentiation des données.
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![ocy](/content/p788061043313147/xxlarge1086.gif) ![vcy](/content/p788061043313147/xxlarge1074.gif) ![acy](/content/p788061043313147/xxlarge1072.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![rcy](/content/p788061043313147/xxlarge1088.gif) ![zcy](/content/p788061043313147/xxlarge1079.gif) ![lcy](/content/p788061043313147/xxlarge1083.gif) ![icy](/content/p788061043313147/xxlarge1080.gif) ![chcy](/content/p788061043313147/xxlarge1095.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![ycy](/content/p788061043313147/xxlarge1099.gif) ![mcy](/content/p788061043313147/xxlarge1084.gif) ![mcy](/content/p788061043313147/xxlarge1084.gif) ![iecy](/content/p788061043313147/xxlarge1077.gif) ![tcy](/content/p788061043313147/xxlarge1090.gif) ![ocy](/content/p788061043313147/xxlarge1086.gif) ![dcy](/content/p788061043313147/xxlarge1076.gif) ![acy](/content/p788061043313147/xxlarge1072.gif) ![mcy](/content/p788061043313147/xxlarge1084.gif) . 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![lcy](/content/p788061043313147/xxlarge1083.gif) ![iecy](/content/p788061043313147/xxlarge1077.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![ycy](/content/p788061043313147/xxlarge1099.gif) ![mcy](/content/p788061043313147/xxlarge1084.gif) ![iecy](/content/p788061043313147/xxlarge1077.gif) ![tcy](/content/p788061043313147/xxlarge1090.gif) ![ocy](/content/p788061043313147/xxlarge1086.gif) ![dcy](/content/p788061043313147/xxlarge1076.gif) , ![ocy](/content/p788061043313147/xxlarge1086.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![ocy](/content/p788061043313147/xxlarge1086.gif) ![vcy](/content/p788061043313147/xxlarge1074.gif) ![acy](/content/p788061043313147/xxlarge1072.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![ycy](/content/p788061043313147/xxlarge1099.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) 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![icy](/content/p788061043313147/xxlarge1080.gif) ![zcy](/content/p788061043313147/xxlarge1079.gif) ![acy](/content/p788061043313147/xxlarge1072.gif) ![tscy](/content/p788061043313147/xxlarge1094.gif) ![icy](/content/p788061043313147/xxlarge1080.gif) ![pcy](/content/p788061043313147/xxlarge1087.gif) ![rcy](/content/p788061043313147/xxlarge1088.gif) ![ocy](/content/p788061043313147/xxlarge1086.gif) ![scy](/content/p788061043313147/xxlarge1089.gif) ![tcy](/content/p788061043313147/xxlarge1090.gif) ![ocy](/content/p788061043313147/xxlarge1086.gif) ![dcy](/content/p788061043313147/xxlarge1076.gif) ![icy](/content/p788061043313147/xxlarge1080.gif) ![fcy](/content/p788061043313147/xxlarge1092.gif) ![fcy](/content/p788061043313147/xxlarge1092.gif) ![iecy](/content/p788061043313147/xxlarge1077.gif) ![rcy](/content/p788061043313147/xxlarge1088.gif) ![iecy](/content/p788061043313147/xxlarge1077.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![tscy](/content/p788061043313147/xxlarge1094.gif) ![icy](/content/p788061043313147/xxlarge1080.gif) ![rcy](/content/p788061043313147/xxlarge1088.gif) ![ocy](/content/p788061043313147/xxlarge1086.gif) ![vcy](/content/p788061043313147/xxlarge1074.gif) ![acy](/content/p788061043313147/xxlarge1072.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![icy](/content/p788061043313147/xxlarge1080.gif) ![acy](/content/p788061043313147/xxlarge1072.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![ncy](/content/p788061043313147/xxlarge1085.gif) ![ycy](/content/p788061043313147/xxlarge1099.gif) .
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