| 不同酸对介孔二氧化硅球表面形貌和介相结构的影响 |
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| 引用本文： | 庞雪蕾,唐芳琼. 不同酸对介孔二氧化硅球表面形貌和介相结构的影响[J]. 无机化学学报, 2004, 20(8): 895-900 |
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| 作者姓名： | 庞雪蕾 唐芳琼 |
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| 作者单位： | 中科院理化技术研究所,北京,100101 |
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| 基金项目： | 国家863计划(No.AA2002302108，2002AA305301)资助项目。 |
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| 摘 要： | 在室温、不同酸性条件下合成出微米级球形介孔二氧化硅材料，通过XRD、SEM以及氮气吸附等手段对介孔二氧化硅材料进行了表征。用TEM跟踪不同反应时间介孔二氧化硅球的形成，对这些球颗粒的合成机理进行了讨论，同时探讨了不同酸性条件下介孔二氧化硅表面形貌和介相结构的变化。
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| 关 键 词： | 介孔二氧化硅 表面形貌 合成机理 介孔二氧化硅球 |
| 修稿时间： | 2004-02-16 |
Effects of Different Acidic Conditions on Surface Patterns and Mesophases of Mesoporous Silica |
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| PANG Xue-Lei and TANG Fang-Qiong. Effects of Different Acidic Conditions on Surface Patterns and Mesophases of Mesoporous Silica[J]. Chinese Journal of Inorganic Chemistry, 2004, 20(8): 895-900 |
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| Authors: | PANG Xue-Lei and TANG Fang-Qiong |
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| Affiliation: | Technical Institute of Physics and Chemistry, Chinese Academy of Science, Beijing 100101 and Technical Institute of Physics and Chemistry, Chinese Academy of Science, Beijing 100101 |
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| Abstract: | Mesoporous silica spheres with diameters in microscale have been synthesized under static acidic conditions by mixed cationic-nonionic surfactant templating. The resulting materials were characterized by X-ray diffraction (XRD), SEM and nitrogenad adsorption. The growth of the micrometer-sized mesoporous silica spheres was examined by transmission electron microscopy (TEM) and a mixed aggregation process was proposed for the formation mechanism of these spheres. The reason that leads to the change of the surface patterns and mesophases of mesoporous silica was discussed. |
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| Keywords: | mesoporous silica surface patterns mechanism mesoporous silica spheres |
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