| 气相色谱-质谱法分析山柰挥发油化学成分 |
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| 引用本文： | 邱琴,刘廷礼,赵怡,赵伟亮. 气相色谱-质谱法分析山柰挥发油化学成分[J]. 理化检验(化学分册), 2000, 36(7): 294-295,298 |
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| 作者姓名： | 邱琴 刘廷礼 赵怡 赵伟亮 |
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| 作者单位： | 1. 山东大学实验中心,济南250100
2. 山东大学化学学院 |
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| 摘 要： | 采用水蒸气蒸馏法从山柰中提取挥发油。采用不同类型的毛细管桩进行分析，找出最佳分析条件，用归一化法测定其质量分数用并用相色谱－质谱法对化学成分进行鉴定。共鉴定了３４种成分，占挥发油总成分的９１％以上。
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| 关 键 词： | 山柰 挥发油 气相色谱－质谱 化学成分分析 中药 |
GC-MS DETERMINATION OF VARIOUS CONSTITUENTS IN KAEMPFERIA GALANGA L |
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| Qiu Qin,Liu Tingli,Zhao Yi,Zhao Weiiiang. GC-MS DETERMINATION OF VARIOUS CONSTITUENTS IN KAEMPFERIA GALANGA L[J]. Physical Testing and Chemical Analysis Part B:Chemical Analgsis, 2000, 36(7): 294-295,298 |
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| Authors: | Qiu Qin Liu Tingli Zhao Yi Zhao Weiiiang |
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| Affiliation: | Qiu Qin,Liu Tingli,Zhao Yi;(Experimental Center, Shandong University Jinan 250100);Zhao Weiiiang;(Institute of Chemistry, Shandong University) |
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| Abstract: | The essential oils in kaempferia galanga L are extracted by the steam distillation method, and determined by GC MS. Various kinds of capillary column are tested and the optimum conditions for analysis are chosen. Thirty four constituents, amounting to 91%, of the kaempferia galanga L are characterized and determined. |
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| Keywords: | Kaempferia galanga L Essential oil GC-MS Capillary gas chromatography |
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