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Synthesis of substituted octahydrochromeno[3,2-<Emphasis Type="Italic">i</Emphasis>]quinazoline-2(1<Emphasis Type="Italic">H</Emphasis>)-thiones
Authors:S I Filimonov  S A Filimonova  A S Shashkov  S I Firgang  G A Stashina
Institution:(1) K. D. Ushinsky Yaroslavl State Pedagogical University, 108 ul. Respublikanskaya, 150000 Yaroslavl, Russian Federation;(2) N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 119991 Moscow, Russian Federation
Abstract:Condensation of 8-arylidenehexahydroquinazoline-2-thiones with di- and trihydroxybenzenes affords the new heterocyclic system, viz., octahydrochromeno3,2-i]quinazoline-2(1H)-thiones, in which the substituents in both the chromane and quinazoline rings can be varied over a wide range. Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 6, pp. 1456–1460, June, 2005.
Keywords:resorcinol  pyrogallol  acid catalysis  hexahydroquinazoline-2-thiones  dihydrobenzopyran (chromane)  two-dimensional NMR spectroscopy
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