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A computer-controlled direct sample insertion device for inductively coupled plasma-mass spectrometry
Authors:Vassilios Karanassios  Gary Horlick
Affiliation:

Department of Chemistry, University of Alberta, Edmonton, Alberta, Canada T6G 2G2

Abstract:
A direct sample insertion (DSI) device has been developed for application to inductively coupled plasma-mass spectrometry (ICP-MS). In a DSI device for use with ICPs, the sample is placed into or onto a probe with subsequent introduction of the sample carrying probe, via the central tube of the ICP torch, into the plasma. A mechanical, stepper-motor driven, computer controlled DSI device and software support system has been designed and developed that can easily be attached to a commercial ICP-MS system (Perkin-Elmer/SClEX Elan). This system allows the direct introduction of microliter volumes of liquids and milligram quantities of powdered/solid samples into the ICP-MS with little or no sample pre-treatment.
Keywords:
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