Synthesis and Characterization of Montmorillonite-Graft-Acrylic Acid Superabsorbent by Using Glow-Discharge Electrolysis Plasma |
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Authors: | Jinzhang Gao Deli Ma Quanfang Lu Yan Li Xingfa Li Wu Yang |
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Institution: | (1) College of Chemistry and Chemical Engineering, Northwest Normal University, 730070 Lanzhou, China |
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Abstract: | Crosslinking graft polymerization of poly acrylic/montmorillonite superabsorbent composite in aqueous solution was prepared
by using glow-discharge electrolysis plasma, in which acrylic acid and acid-activated montmorillonite were used as starting
materials, N,N-methylenebisacrylamide as a crosslinking agent. To optimize the synthetic conditions, seven important parameters of the graft-polymerization
were examined in detail, such as the discharge voltage, discharge time, the neutralization of acrylic acid, post polymerization
temperature, amounts of crosslinking agent, montmorillonite and acrylic acid used in this study. The structure, thermal stability
and morphology of product were characterized by Fourier transform infrared spectroscopy, thermogravimetric analysis, scanning
electron microscopy, respectively. The absorbency of poly acrylic/montmorillonite superabsorbent was examined to yield the
following results: 1,834 g/g for distilled water, 116 g/g for 0.05 mol/L and 75 g/g for 0.15 mol/L sodium chloride solution.
Such excellent character could be important to use in many fields, for example, in agricultural and horticultural applications. |
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