| 孕甾-3,6,20-三肟和孕甾-6,20-二酮-3-肟的合成 |
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| 引用本文： | 张晓佳,范磊,李月骅,崔建国. 孕甾-3,6,20-三肟和孕甾-6,20-二酮-3-肟的合成[J]. 化学研究与应用, 2009, 21(5) |
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| 作者姓名： | 张晓佳 范磊 李月骅 崔建国 |
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| 作者单位： | 广西师范学院化学系,广西,南宁,530001;广西师范学院化学系,广西,南宁,530001;广西师范学院化学系,广西,南宁,530001;广西师范学院化学系,广西,南宁,530001 |
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| 基金项目： | 国家自然科学基金，广西自治区科学基金，广西教育厅基金 |
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| 摘 要： | 自上世纪六十年代兴起海洋天然产物的研究热潮以来,科学家们已从海洋生物中分离得到许多结构新颖、具有一系列极强生理活性的天然产物[1-3].
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| 关 键 词： | 孕烯醇酮 孕甾-3 6 20-三肟 合成 |
Synthesis of pregna-3,6,20-trioxime and pregna-6,20-dione-3-oxime |
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| ZHANG Xiao-jia,FAN Lei,LI Yue-hua,CUI Jian-guo. Synthesis of pregna-3,6,20-trioxime and pregna-6,20-dione-3-oxime[J]. Chemical Research and Application, 2009, 21(5) |
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| Authors: | ZHANG Xiao-jia FAN Lei LI Yue-hua CUI Jian-guo |
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| Affiliation: | Department of Chemistry;Guangxi Teachers Education University;Nanning 530001;China |
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| Abstract: | Pregna-3,6,20-trioxime and its analog,pregna-6,20-dione-3-oxime were synthesized from pregnenolone by the oxidation of PCC,reduction of NaBH4,oxidation of Jone's agent and oximation in four-step reaction.Their structures were characterized by NMR and IR. |
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| Keywords: | pregnenolone pregna-3 6 20-trioxime synthesis |
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