Gas-chromatographic determination of aliphatic amines in natural surface water and wastewater |
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Authors: | N V Kuz’mina F F Khizbullin T Ya Gadomskii V N Maistrenko |
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Institution: | (1) Research Institute of Life Safety of the Republic of Bashkortostan, ul. 8 Marta 12/1, Ufa, 450005, Bashkortostan, Russia;(2) Center for Ecological Research, Academy of Sciences of the Republic of Bashkortostan, ul. 8 Marta 12/1, Ufa, 450005, Bashkortostan, Russia |
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Abstract: | A procedure was developed for the gas-chromatographic determination of aliphatic amines C7–C20 with prederivatization by N-methyl-bis(trifluoroacetamide), in the concentration range of natural surface water, to 10?4-1 mg/L, and wastewater, to 10?3-1 mg/L. The conditions were optimized for the extraction preconcentration of aliphatic amines with toluene from natural surface water and wastewater. The detection limit for aliphatic amines at a signal-to-noise ratio of 3: 1 was 50 ng/L. |
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