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Measurement of J-couplings between spin-(1/2) and quadrupolar nuclei by frequency selective solid-state NMR |
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| Authors: | Amoureux J-P Trebosc J Wiench J W Massiot D Pruski M |
| Institution: | LCPS, CNRS-8012, Université de Lille-1, 59652 Villeneuve d'Ascq, France. |
| Abstract: | We report a REDOR-based scheme for the measurement of heteronuclear J-couplings in solid samples with well defined structure, containing spin-12 and quadrupolar nuclei, which can be used with selective RF irradiation to target a specific spin pair, and which provides direct information about the number of coupled spins. |
| Keywords: | Solid-state NMR of quadrupolar nuclei J-coupling FS– J-RES Aluminophosphates VPI5 |
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