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Synthesis and Crystal Structure of exo-4-(3,4-Dichlorophenyl)-8-ethyl-3,3a,4,5,8, 12d-hexahydro-2H-furo[3,2-c]indolo[3,2-f]quinoline
引用本文:王树良,周洁,杨科,王香善,屠树江. Synthesis and Crystal Structure of exo-4-(3,4-Dichlorophenyl)-8-ethyl-3,3a,4,5,8, 12d-hexahydro-2H-furo[3,2-c]indolo[3,2-f]quinoline[J]. 结构化学, 2011, 30(9): 1275-1278
作者姓名:王树良  周洁  杨科  王香善  屠树江
作者单位:School of Chemistry and Chemical Engineering;Xuzhou Normal University;
基金项目:supported by the National Natural Science Foundation of China (20802061); Natural Science Foundation of the Education Committee of Jiangsu Province (08KJD150019);Qinglan Project (08QLT001) of the Education Committee of Jiangsu Province
摘    要:The title compound exo-4-(3,4-dichlorophenyl)-8-ethyl-3,3a,4,5,8,12d-hexahydro-2H-furo[3,2-c]indolo[3,2-f]quinoline (C25H22Cl2N2O, Mr = 437.35) was synthesized and crystallized. The crystal belongs to tetragonal, space group I4(1)/a with a = 17.4903(3), b = 17.4903(3), c = 28.3403(5) , Z = 16, V = 8669.6(3) 3, Dc = 1.340 g·cm-3, μ(MoKɑ) = 0.319 mm-1, F(000) = 3648, R = 0.0429 and wR = 0.711 for 2714 observed reflections I > 2σ(I). X-ray analysis reveals that atoms C(1), C(2), C(3), C(4), C(5) and N(1) on the new pyridine ring are slightly distorted, forming a distorted boat conformation.

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Synthesis and Crystal Structure of exo-4-(3,4-Dichlorophenyl)-8-ethyl-3,3a,4,5,8, 12d-hexahydro-2H-furo[3,2-c]indolo[3,2-f]quinoline
WANG Shu-Liang , ZHOU Jie , YANG Ke , WANG Xiang-Shan , TU Shu-Jiang. Synthesis and Crystal Structure of exo-4-(3,4-Dichlorophenyl)-8-ethyl-3,3a,4,5,8, 12d-hexahydro-2H-furo[3,2-c]indolo[3,2-f]quinoline[J]. Chinese Journal of Structural Chemistry, 2011, 30(9): 1275-1278
Authors:WANG Shu-Liang    ZHOU Jie    YANG Ke    WANG Xiang-Shan    TU Shu-Jiang
Affiliation:School of Chemistry and Chemical Engineering, Xuzhou Normal University, Xuzhou 221116, China
Abstract:The title compound exo-4-(3,4-dichlorophenyl)-8-ethyl-3,3a,4,5,8,12d-hexahydro-2H-furo[3,2-c]indolo[3,2-f]quinoline (C25H22Cl2N2O, Mr = 437.35) was synthesized and crystallized. The crystal belongs to tetragonal, space group I4(1)/a with a = 17.4903(3), b = 17.4903(3), c = 28.3403(5) , Z = 16, V = 8669.6(3) 3, Dc = 1.340 g·cm-3, μ(MoKɑ) = 0.319 mm-1, F(000) = 3648, R = 0.0429 and wR = 0.711 for 2714 observed reflections I > 2σ(I). X-ray analysis reveals that atoms C(1), C(2), C(3), C(4), C(5) and N(1) on the new pyridine ring are slightly distorted, forming a distorted boat conformation.
Keywords:crystal structure  indolo[3  2-f]quinoline  NMR  
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