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Saucer-and Rod-like WO_3 3-D Microstructures:Synthesis,Characterization,and Optical Properties
Authors:CHEN Lin  YAN Ting-Jiang  ZHENG Jing  LI Li-Ping
Institution:1. Key Laboratory of Optoelectronic Materials Chemistry and Physics, Fujian Institute ofResearch on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002, China
2. State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002, China
Abstract:Three-dimensional(3-D)saucer-and rod-like WO3 microstructures have been synthesized by a simple hydrothermal route using tartaric acid as the assistant agent.X-ray powder diffraction(XRD)patterns indicate that the as-prepared samples are the pure hexagonal phase WO3.The morphologies are characterized by scanning electron microscope(SEM)and are found to be highly sensitized to the reaction temperature.A probable formation mechanism of the WO3 microstructures from saucer-like at low temperatures to rod-like a...
Keywords:hydrothermal  three-dimensional  adsorbed water  electronic structure  
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