| 新药盐酸美利曲辛的有机波谱分析 |
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| 引用本文： | 许崇德,郑艳萍,孙秀燕.新药盐酸美利曲辛的有机波谱分析[J].分析测试学报,2007,26(2):255-257. |
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| 作者姓名： | 许崇德 郑艳萍 孙秀燕 |
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| 作者单位： | 1. 日照市人民医院,山东,日照,276800
2. 烟台大学,药学院,山东,烟台,264005 |
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| 摘 要： | 采用核磁共振波谱(NMR)、电喷雾质谱(ESI MS)、紫外(UV)、红外(IR)吸收光谱等技术确证新药盐酸美利曲辛的分子结构;应用NOE谱技术确定盐酸美利曲辛分子中芳香氢的各自化学位移信号;解释该结构在NMR、ESI MS、UV、IR等谱图中的特征吸收峰、共振峰及特征离子的一一对应归属.
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| 关 键 词： | 盐酸美利曲辛 核磁共振波谱 电喷雾质谱 红外光谱 紫外光谱 结构确证 |
| 文章编号： | 1004-4957（2007）02-0255-03 |
| 收稿时间： | 2006-03-04 |
| 修稿时间： | 2006-09-15 |
Stuctural Identification of Nelitracen Hydrocholride by Spectroscopic Techniques |
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| XU Chong-de,ZHENG Yan-ping,SUN Xiu-yan.Stuctural Identification of Nelitracen Hydrocholride by Spectroscopic Techniques[J].Journal of Instrumental Analysis,2007,26(2):255-257. |
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| Authors: | XU Chong-de ZHENG Yan-ping SUN Xiu-yan |
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| Abstract: | The molecular structure of nelitracen hydrocholride was identified by a series of spectroscopic techniques including NMR, ESI MS, UV and IR. The signal of the chemical shifts of aromatic hydrogen in nelitracen hydrocholride molecule was determined by NOE spectroscopic technique. The corresponding attribution of the characteristic absorption peaks, the resonant peak and the characteristic ions in NMR, ESI MS, UV and IR spectra were explained, respectively. |
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| Keywords: | Nelitracen hydrocholride NMR ESI MS IR UV Structural identification |
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