Synthesis of a singly bridged resorcinarene-dimer by Mannich reaction with N,N′-diethylethylenediamine and formaldehyde: self-inclusion of bridging diazahexamethylene unit in methanol |
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Authors: | Osamu Morikawa |
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Institution: | Department of Materials Science, Faculty of Engineering, Tottori University, 4-101 Koyama-minami, Tottori 680-8552, Japan |
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Abstract: | Mannich reaction of resorcin4]arene with N,N′-diethylethylenediamine and formaldehyde produced a singly bridged resorcinarene-dimer bearing sixteen hydroxyl groups at their peripheral positions, which exists in a closed capsular conformation including the diazahexamethylene bridge chain between the two resorcinarene units in CD3OD. |
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Keywords: | Self-inclusion Capsule Resorcin[4]arene dimer Mannich reaction |
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