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Complete assignments of 1H and 13C NMR spectroscopic data for three new stigmastane glycosides from Vernonia cumingiana
Authors:Maorong Suo  Junshan Yang
Institution:Institute of Medicinal Plant Development, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing, 100094, China
Abstract:Three new steroidal saponins, Vernoniosides S1 ( 1 ), Vernoniosides S2 ( 2 ) and Vernoniosides S3 ( 3 ) were isolated from the stem of Vernonia cumingian. Their chemical structures were elucidated on the basis of MS, NMR spectroscopic and chemical analysis. Complete assignment of 1H and 13C NMR spectroscopic data were achieved by 1D and 2D NMR experiments (HMQC, HMBC, ROESY). Copyright © 2008 John Wiley & Sons, Ltd.
Keywords:NMR  1H NMR  13C NMR  1D NMR  2D NMR  Vernonia cumingian  steroidal saponins  Vernoniosides S1  Vernoniosides S2  Vernoniosides S3
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