Sintering
of hydroxyapatite lath-like powders |
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Authors: | G C Koumoulidis C C Trapalis T C Vaimakis |
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Institution: | (1) Department of Chemistry, University of Ioannina, Ioannina, Greece, 1186, 451 10;(2) Demokritos’ National Center for Scientific Research, Institute of Materials Science, Athens, Greece, 153 10 |
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Abstract: | Hydroxyapatite
powders, which consisted of lath-like single-crystalline particles, were calcined
at two different temperatures. Green and calcined powders were used for sintering
HAp ceramic samples under uniaxial pressing. Powders and sintered samples
were studied using various analytical techniques in order to determine how
calcination affects the particle properties and the sintering behavior of
HAp powders. It was found that calcination decreases the particles length
and changes the particles morphology from lath-like to spherical shape. The
relative density increases with increasing calcination temperature and aging
time. It was found that long aging time favor the formation of thermally stable
HAp particles, whereas a shorter one results in the formation of β-calcium
phosphate during thermal treatment. Sintering of compacted powders begins
at temperatures greater than 900°C, with a trend to increase the onset
temperature as the calcination temperature is increased. |
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Keywords: | apatite-D biomedical applications-E calcination-A sintering-B whiskers-C |
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