| 超声技术合成1,5-二-(4-羟基苯基)-1,4-戊二烯-3-酮 |
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| 引用本文： | 谭冶,严石静,李立忠,申凤善,李香丹. 超声技术合成1,5-二-(4-羟基苯基)-1,4-戊二烯-3-酮[J]. 分子科学学报, 2012, 28(3): 252-255 |
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| 作者姓名： | 谭冶 严石静 李立忠 申凤善 李香丹 |
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| 作者单位： | 1. 中南民族大学化学与材料科学学院,湖北武汉,430074
2. 延边大学理学院,吉林延吉,133002 |
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| 基金项目： | 湖北省自然科学基金资助项目 |
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| 摘 要： | 利用对羟基苯甲醛和丙酮为原料,以氯化氢气体为催化剂,超声波辐射下成功合成了1,5-二-(4-羟基苯基)-1,4-戊二烯3-酮(HPD).与传统方法相比,该方法具有反应时间短,操作简便及产率高等优点,并讨论了影响产率的因素.
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| 关 键 词： | 1,5-二-(4-羟基苯基)-1,4-戊二烯-3-酮(HPD) 超声 |
Ultrasonic synthesis of 1,5-2-(4-hydroxyphenyl)-1,4-pentadiene-3-one |
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| TAN Ye , YAN Shi-jing , LI Li-zhong , SHEN Feng-shang , LI Xiang-dan. Ultrasonic synthesis of 1,5-2-(4-hydroxyphenyl)-1,4-pentadiene-3-one[J]. Journal of Molecular Science, 2012, 28(3): 252-255 |
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| Authors: | TAN Ye YAN Shi-jing LI Li-zhong SHEN Feng-shang LI Xiang-dan |
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| Affiliation: | 1(1.College of Chemistry and Materials Science,South Central University for Nationalities,Wuhan 430074,China; 2.Science College of Yanbian University,Yanji 133002,China) |
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| Abstract: | 1,5-2-(4-hydroxyphenyl)-1,4-pentadiene-3-one(HPD) was successfully synthesized by the condensation of acetone and p-hydroxybenzaldehyde under ultrasound irradiation in the presence of HCl gas as a catalyst.Compared with conventional methods,it provided a convenient procedure with shorter reaction time and higher yields.The factors influencing the product were discussed. |
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| Keywords: | 1,5-2-(4-hydroxyphenyl)-1,4-pentadiene-3-one(HPD) ultrasonic |
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