A synthetic study towards the PSA1 tetrasaccharide repeating unit |
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| Authors: | Leendert J van den Bos Tom Provoost Herman S Overkleeft |
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| Institution: | a Leiden Institute of Chemistry, Leiden University, PO Box 9502, 2300 RA Leiden, The Netherlands
b Avantium Technologies, Zekeringstraat 29, 1014 BV, Amsterdam, The Netherlands |
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| Abstract: | A synthetic study to the protected tetrasaccharide repeating unit of zwitterionic polysaccharide PSA1 using 1-thio, 1-seleno and 1-hydroxyl functionalized donor glycosides is presented. The ABC trisaccharide part was successfully assembled using an iterative dehydrative glycosylation protocol. |
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